ｻﾝﾌﾟﾙ: '191024 Sample ﾌｧｲﾙ名: 191024 10μg アスコルビン.FD3 分析日時: '10:02:50, 10/24/2019 ｵﾍﾟﾚｰﾀ: 筑波大学 ｺﾒﾝﾄ: ' 光度計 ﾓﾃﾞﾙ: F-7000形分光蛍光光度計 ｼﾘｱﾙ No.: 2357-015 ROM Ver.: 5J14000 06 装置条件 測定ﾓｰﾄﾞ: 3次元 ﾃﾞｰﾀﾓｰﾄﾞ: 蛍光 励起開始波長: 200.0 nm 励起終了波長: 500.0 nm 励起側ｻﾝﾌﾟﾘﾝｸﾞ間隔: 10.0 nm 蛍光開始波長: 200.0 nm 蛍光終了波長: 700.0 nm 蛍光側ｻﾝﾌﾟﾘﾝｸﾞ間隔: 10.0 nm ｽｷｬﾝｽﾋﾟｰﾄﾞ: 30000 nm/min 励起側ｽﾘｯﾄ: 5.0 nm 蛍光側ｽﾘｯﾄ: 5.0 nm ﾎﾄﾏﾙ電圧: 700 V ﾚｽﾎﾟﾝｽ: 自動 ｽﾍﾟｸﾄﾙ補正: On ｼｬｯﾀ制御: On 等高線間隔: 50.000 装置関数 励起側(200〜500nm) ｽﾘｯﾄ：5.0/20.0nm ﾎﾄﾏﾙ電圧：400V 蛍光側(200〜500nm) ｽﾘｯﾄ：5.0/20.0nm ﾎﾄﾏﾙ電圧：250V 蛍光側(500〜900nm) ｽﾘｯﾄ：---/5.0nm ﾎﾄﾏﾙ電圧：400V 励起側(500〜900nm) ｽﾘｯﾄ：5.0/5.0nm ﾎﾄﾏﾙ電圧：350V ﾃﾞｰﾀﾘｽﾄ 200.000 210.000 220.000 230.000 240.000 250.000 260.000 270.000 280.000 290.000 300.000 310.000 320.000 330.000 340.000 350.000 360.000 370.000 380.000 390.000 400.000 410.000 420.000 430.000 440.000 450.000 460.000 470.000 480.000 490.000 500.000 200.0 9999.9 3222 59.68 30.14 15.64 20.94 21.61 25.09 23.92 27.73 28.62 26.78 23.54 20.18 20.07 16.06 15.84 13.08 13.39 11.41 37.88 38.34 7.659 7.166 6.146 4.622 4.494 3.707 3.797 2.482 3.238 210.0 607.3 9999.9 2547 26.62 17.12 13.29 15.80 14.32 15.35 17.03 17.33 15.55 14.90 12.81 11.30 10.45 9.544 8.848 7.521 6.799 6.341 9.930 52.29 45.80 4.143 3.250 2.917 2.176 2.370 1.839 1.910 220.0 65.98 643.0 9999.9 2679 20.75 13.58 12.66 11.34 12.28 11.69 11.33 11.93 10.67 9.076 7.612 6.999 6.181 6.073 5.013 4.824 4.247 3.824 4.966 9.971 76.59 66.31 3.677 1.743 1.569 1.539 1.318 230.0 75.97 136.0 679.7 9999.9 3095 24.10 16.11 12.30 10.52 11.43 10.63 10.23 8.926 7.594 6.855 6.224 5.401 5.165 4.375 3.912 3.307 2.833 2.381 2.524 4.942 13.94 140.1 103.7 4.442 1.266 1.377 240.0 54.74 99.03 129.8 708.3 9999.9 3635 26.09 16.60 12.81 11.63 11.54 9.553 8.218 7.143 6.809 6.073 5.052 4.086 4.096 3.553 2.923 2.483 2.316 1.704 2.025 2.188 6.795 25.99 285.6 210.6 6.088 250.0 132.3 108.6 71.40 117.9 762.6 9999.9 4570 30.22 17.97 14.41 12.04 10.28 8.883 7.320 6.703 5.619 5.058 4.772 3.763 3.172 2.926 2.623 2.227 2.082 2.045 1.625 1.610 2.267 12.25 53.86 542.4 260.0 218.1 124.1 99.92 61.81 113.2 826.3 9999.9 5231 36.12 22.32 16.66 12.12 9.172 8.463 7.106 6.315 5.095 5.163 4.152 3.311 2.704 2.797 2.552 2.297 1.987 1.728 1.424 1.427 1.994 3.405 22.32 270.0 307.1 206.6 116.5 79.33 60.69 115.1 857.7 9999.9 5752 44.47 26.73 16.98 12.01 10.12 8.020 6.832 6.144 5.202 4.571 3.710 3.244 2.764 2.697 2.075 2.177 1.950 1.711 1.406 1.535 1.641 2.481 280.0 484.9 278.8 193.3 88.14 54.80 65.06 116.5 986.5 9999.9 5167 53.54 28.64 18.09 12.78 9.852 7.918 6.798 5.740 5.108 4.229 3.906 3.377 3.243 2.846 2.332 2.200 2.065 1.694 1.818 1.786 1.886 290.0 858.4 479.3 310.7 195.1 109.2 81.83 129.2 225.5 1161 9999.9 5081 61.16 32.17 20.54 13.95 10.48 8.643 7.228 6.704 5.345 4.716 4.267 3.607 3.515 3.106 2.880 2.537 2.186 2.677 2.281 2.297 300.0 1167 787.7 492.2 382.1 228.1 172.7 256.4 412.8 496.1 1529 9999.9 4609 70.06 35.19 22.00 14.58 11.47 9.318 7.586 6.796 6.398 5.731 4.771 4.175 3.915 3.704 3.650 3.013 2.993 3.107 3.447 310.0 1332 973.7 616.8 482.4 291.7 230.0 356.1 511.8 632.1 441.9 1432 9999.9 4523 77.26 39.69 25.18 15.79 12.61 10.05 8.073 6.968 6.206 5.991 5.185 4.996 4.172 4.584 3.874 3.856 3.594 4.110 320.0 1544 1019 780.7 563.2 297.1 256.4 380.2 549.2 622.2 490.1 228.3 1396 9999.9 4599 81.03 41.03 26.72 17.29 12.69 10.57 8.941 7.926 6.680 6.312 5.452 4.964 4.798 4.195 4.513 4.112 4.551 330.0 1448 1077 796.7 587.5 311.6 253.2 365.5 500.7 574.0 438.5 210.3 175.3 1181 9999.9 4554 81.61 42.84 26.77 17.82 13.04 10.36 8.489 7.990 7.494 6.546 5.751 4.891 4.757 4.925 4.372 4.709 340.0 1742 1043 886.8 673.7 364.2 287.0 337.1 423.9 485.3 408.2 183.8 130.9 165.4 1021 9999.9 4462 83.11 41.83 25.76 17.58 12.42 10.48 8.833 7.977 7.012 6.658 5.733 5.223 5.043 5.198 5.028 350.0 1883 1126 817.5 613.6 403.1 282.2 285.9 345.2 394.0 346.1 159.2 121.9 111.7 150.0 1003 9999.9 4481 79.28 39.96 25.78 16.68 13.03 10.44 8.891 7.858 7.611 6.733 5.367 5.104 4.793 5.628 360.0 1965 1259 770.8 558.6 369.7 260.8 248.4 270.4 298.7 267.5 139.1 103.8 121.8 96.91 137.6 903.9 9999.9 4395 76.04 38.40 24.38 17.00 12.48 10.14 8.702 7.424 6.833 5.529 5.790 4.911 4.865 370.0 1922 1211 719.9 499.1 314.0 217.8 199.2 211.6 224.7 213.7 121.9 97.98 96.86 112.2 85.65 125.6 831.5 9999.9 4331 74.86 37.20 22.96 16.60 11.32 9.885 7.641 7.234 6.035 6.207 5.331 5.217 380.0 1646 1123 617.3 434.9 284.2 202.7 159.4 169.9 178.2 163.9 111.3 93.96 91.35 87.17 92.25 74.56 117.8 810.4 9999.9 4280 70.05 34.91 23.00 15.04 10.90 9.063 7.621 6.401 6.474 6.088 5.455 390.0 7530 1082 629.5 407.9 247.4 180.1 146.4 148.6 145.5 132.7 97.92 89.92 88.26 82.60 82.14 76.86 73.14 113.7 797.3 9999.9 4372 69.75 33.67 21.55 14.84 10.34 8.460 7.081 6.418 5.459 5.848 400.0 9999.9 983.6 611.6 344.0 232.5 169.2 130.2 127.2 131.7 113.9 87.05 85.39 85.01 79.53 74.94 81.04 71.17 69.28 112.6 789.8 9999.9 4411 66.53 30.73 19.39 13.39 9.805 7.880 7.206 6.391 5.270 410.0 3350 9999.9 488.2 350.7 216.9 145.9 118.1 113.5 115.9 97.91 82.31 78.03 78.66 75.90 70.59 67.59 76.75 60.15 63.08 100.7 732.3 9999.9 4550 61.75 29.45 18.35 12.50 9.198 7.492 6.758 6.124 420.0 1595 9999.9 510.4 303.3 196.4 137.5 106.4 103.0 103.1 87.94 76.29 75.45 73.07 68.25 66.89 65.16 64.66 68.55 56.12 55.72 85.79 708.3 9999.9 4441 57.74 27.79 17.42 11.41 9.300 7.120 7.164 430.0 1337 4609 9999.9 273.1 193.0 134.1 103.1 98.52 96.08 80.28 69.84 69.39 68.06 66.80 63.75 62.43 56.87 55.13 53.24 45.15 43.91 82.91 672.8 9999.9 4253 54.05 25.83 16.35 11.39 9.102 7.549 440.0 1156 949.3 9999.9 265.5 176.9 141.5 109.7 91.80 89.26 78.64 68.11 65.55 62.90 62.24 60.42 62.13 55.75 49.99 50.64 44.41 37.91 42.65 75.65 714.7 9999.9 4024 50.89 23.27 16.46 10.68 9.000 450.0 1229 866.9 6355 9999.9 180.0 143.5 107.3 86.17 83.42 71.87 63.08 60.01 57.17 58.86 57.71 60.12 53.98 46.87 44.19 48.14 36.89 36.05 38.13 76.76 699.7 9999.9 3887 47.29 23.65 15.11 10.96 460.0 1260 769.6 718.8 9999.9 200.4 154.4 108.7 85.84 82.11 74.33 62.01 58.10 56.57 54.36 54.85 56.21 51.86 45.06 42.62 39.23 40.57 33.23 33.33 36.64 73.73 644.9 9999.9 3940 50.08 22.82 16.22 470.0 1117 909.9 462.2 7214 9999.9 165.4 112.7 87.25 80.77 71.61 61.97 56.37 54.11 50.65 52.62 52.85 50.69 43.75 39.99 36.81 35.52 36.82 37.24 38.20 39.82 69.01 648.2 9999.9 4700 47.55 25.40 480.0 1123 679.7 395.6 495.4 9999.9 197.5 109.0 80.75 77.86 74.50 62.99 56.45 52.05 49.32 47.53 50.29 44.22 40.27 38.19 33.97 31.18 32.97 28.95 29.19 29.06 30.71 63.00 572.0 9999.9 4723 48.90 490.0 985.6 602.6 327.9 237.8 8926 9999.9 112.1 80.92 69.68 69.27 59.88 55.70 48.75 45.92 45.06 44.31 39.50 34.72 33.04 30.81 29.20 26.62 28.92 25.83 24.95 24.66 26.51 53.98 554.4 9999.9 5360 500.0 700.6 576.5 290.6 212.2 499.3 9999.9 165.4 80.20 69.19 63.57 56.16 53.98 47.02 42.42 40.94 39.07 36.30 30.42 29.67 28.48 26.91 26.41 23.59 26.99 22.39 22.80 22.77 23.24 51.40 552.6 9999.9 510.0 754.9 457.4 261.1 175.3 147.0 9999.9 9999.9 91.14 73.05 59.88 56.06 50.97 48.44 41.17 40.01 36.48 31.60 29.45 26.30 24.71 24.82 23.03 21.28 21.06 22.47 18.69 18.79 18.55 21.56 49.32 533.6 520.0 747.5 460.6 284.5 158.3 141.5 523.0 9999.9 154.6 79.36 61.82 56.18 51.64 47.86 43.48 38.64 35.94 32.49 26.19 23.74 21.80 21.42 21.42 19.13 18.95 19.37 18.44 18.11 15.70 18.03 21.36 47.30 530.0 652.3 391.4 240.6 134.9 109.6 147.2 9999.9 9999.9 92.65 68.84 55.37 52.23 46.53 44.76 36.67 34.28 30.49 24.99 24.01 20.93 18.66 19.24 19.25 18.32 16.91 17.67 15.86 14.33 14.64 16.52 20.69 540.0 654.7 407.0 247.8 135.8 109.2 126.4 507.8 9999.9 181.9 81.81 65.06 52.32 47.35 42.89 39.18 35.86 29.12 24.55 21.23 20.61 19.11 16.81 16.33 17.10 15.99 14.68 15.92 13.28 13.54 14.59 15.61 550.0 559.3 439.7 243.9 136.0 86.09 117.9 125.0 9999.9 9999.9 99.87 76.04 57.27 47.57 42.96 38.75 34.06 29.87 24.13 23.03 19.69 18.78 16.00 14.80 14.15 15.79 14.59 14.29 12.73 12.85 14.06 13.97 560.0 742.2 421.0 285.7 136.6 84.37 89.58 92.61 505.3 9999.9 180.3 91.22 62.41 50.08 46.40 39.66 34.88 30.35 26.48 21.08 19.63 18.13 15.91 14.61 13.37 13.16 13.67 12.90 13.86 11.08 11.98 13.34 570.0 646.9 458.5 275.5 124.9 79.22 85.62 107.7 124.0 9999.9 9999.9 113.8 77.04 54.34 44.54 38.26 35.87 31.93 27.11 25.37 18.35 16.50 15.74 14.38 12.75 12.79 11.47 12.99 11.35 12.03 11.66 13.16 580.0 1042 508.8 325.5 166.6 105.7 79.64 104.3 133.4 562.9 9999.9 216.1 92.83 62.24 49.43 40.42 37.18 31.75 26.73 24.66 23.30 16.71 16.03 14.21 13.50 11.08 11.57 10.18 10.76 12.16 11.31 11.89 590.0 4250 544.4 282.1 173.2 121.3 100.3 118.0 175.1 218.0 9999.9 9999.9 116.5 79.37 55.98 46.37 38.05 31.87 28.47 25.36 23.36 19.81 17.41 14.24 13.42 11.92 11.18 10.19 9.519 10.80 11.95 10.88 600.0 6956 609.8 347.7 225.2 131.6 116.8 150.8 217.7 241.9 602.0 9999.9 211.1 93.17 62.19 47.78 37.85 35.60 28.47 26.36 22.61 23.40 17.41 15.01 13.74 11.81 11.03 10.62 9.963 9.231 9.494 12.37 610.0 3279 740.6 287.4 244.1 153.2 111.4 158.2 231.7 267.5 221.8 9999.9 9999.9 117.5 77.81 54.48 43.70 35.33 28.90 27.18 21.75 20.54 22.99 16.45 13.34 13.28 11.29 9.502 8.726 8.285 8.486 10.49 620.0 1007 3612 329.7 269.4 151.6 128.0 162.9 233.2 279.6 205.2 537.5 9999.9 207.1 91.54 62.14 47.04 39.11 32.57 28.74 23.49 21.96 21.00 17.54 16.11 11.63 12.36 10.08 8.743 8.934 8.336 9.179 630.0 816.4 8004 419.2 266.5 161.7 133.6 182.2 228.0 273.8 208.2 152.9 9999.9 9999.9 119.7 77.73 54.85 45.13 37.13 31.64 25.65 22.85 19.76 28.73 17.43 13.57 12.23 9.698 9.373 9.610 8.183 7.789 640.0 705.1 5174 477.8 259.0 140.3 120.9 174.1 236.3 268.0 224.7 133.7 536.4 9999.9 213.2 93.62 67.15 48.51 38.42 32.62 28.71 25.43 21.36 19.74 25.26 14.87 13.72 12.11 9.249 8.572 7.511 8.689 650.0 1252 824.3 3617 235.0 126.3 124.2 161.7 221.4 242.3 207.8 130.6 151.2 9999.9 9999.9 117.4 82.42 60.49 47.05 38.86 30.21 26.01 24.93 20.29 28.57 18.02 15.34 12.08 10.42 8.765 9.124 7.766 660.0 1017 615.1 9999.9 254.7 141.9 124.1 159.5 214.4 224.0 198.6 136.4 117.9 548.7 9999.9 203.8 91.93 70.00 54.25 46.39 33.95 31.14 28.48 21.90 20.96 41.11 16.89 13.50 13.05 9.072 9.114 7.968 670.0 814.9 824.2 7501 421.7 157.6 113.3 149.2 182.1 224.9 195.9 139.0 112.8 148.1 9999.9 9999.9 123.3 83.25 61.26 48.34 43.13 33.21 29.18 26.19 23.23 21.00 35.37 15.93 12.83 8.818 9.966 7.764 680.0 1231 678.4 966.9 4806 165.7 134.1 162.3 181.6 213.8 189.4 127.8 114.7 122.8 556.1 9999.9 205.5 99.28 72.68 55.87 47.27 42.70 34.25 29.22 26.12 21.07 42.52 19.80 13.69 11.70 10.67 10.17 690.0 1103 750.5 370.4 9999.9 159.9 130.6 172.4 173.6 188.3 184.5 121.6 118.5 119.0 156.4 9999.9 9999.9 134.3 84.10 67.97 50.10 46.73 39.73 31.76 29.21 24.08 23.41 75.83 15.49 13.23 11.95 11.94 700.0 1007 571.0 521.1 9999.9 399.8 129.6 137.1 152.3 165.0 169.5 108.1 110.3 110.2 123.0 569.0 9999.9 211.1 100.8 70.45 64.58 48.79 43.43 37.11 29.86 26.87 23.90 25.65 54.46 13.74 12.31 12.17